Molecular structure of (+/-)-5-benzylamino-endo-tricylo[5.2.1.0(2,6)]dec-4-en-3-one
de Gelder R, Smits JMM, Bakkeren FJAD, Klunder AJH
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY 27 (11): 677-679 NOV 1997

Abstract:
The crystal and molecular structure of (+/-)-5-benzylamino-endo-tricyclo[5.2.1.0(2,6)]dec-4-en-3-one is described. The X-ray analysis revealed that the reduction of the norbomene double bond is an important process in the irradiation of the used enaminones. The structure was solved by direct methods and refined by least squares methods to R-1 = 0.0468 for 2070 reflections (with I > 2 sigma(I)). Crystal data: C17H19NO, Orthorhombic, space group Pbcn, a = 40.695 (1), b = 6.6928 (1), c = 10.2378(4)Angstrom, V = 2788.44(14)Angstrom(3), Z = 8.